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In-situ Differential Electrochemical Mass Spectrometer(For Electrocatalysis Application)

In-situ Differential Electrochemical Mass Spectrometry (Probe type)


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In-situ Differential Electrochemical Mass Spectrometry (Probe type)

Differential Electrochemical Mass Spectrometer(DEMS) is an in-situ electrochemical method. By detecting volatile products, it can obtain qualitative and quantitative information of the interface and become an indispensable tool for studying the mechanism of electrochemical reactions. The DEMS system connects the Electrochemical Reaction Device with the Mass Spectrometer. Volatile products generated by the electrochemical reaction and then entered the vacuum system pipeline of the Mass Spectrometer from the hydrophobic membrane interface, and the current of the different ions change with time is obtained by the Mass Spectrometer. In the study of electrochemical reaction mechanics, cyclic voltammetry(CV) is a more commonly used electrochemical method.Richelectrochemical information can be obtained from the obtained CV graphics. Therefore, CV is frequently used in DEMS research.When using DEMS for electrochemical research, the ion current signal of the volatile product generated during the CV sweep is detected by the Mass Spectrometer over time, and the ion current changes with the potential (MSCV) are obtained by the transformation of the time axial to potential axis. MSCV provides more comprehensive and in-depth information for the study of electrocatalytic reaction mechanism.

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Fig. 1:  Working principle ofprobe type In-situ Differential Electrochemical Mass Spectrometer


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Fig. 2Liquidphase conversion of ethanol using Rh/C catalyst. (b, c) liquid-phase product analysis using online DEMS. J. Am. Chem. Soc. 2019DOI: 10.1021/jacs.8b13115

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Fig. 3Simultaneouslyrecorded cyclic voltammogram (CV) (a) mass spectrometric CV (MSCV) for m/z = 91 (b)MSCVfor m/z = 58 

(c) on a carbon paper cathode in 0.1 M DMF + 0.1 M Bu4PBF4 at a scan rate of 5 mV/s, and proposed reaction mechanism

 (d)ACSCatal. 2019, 9, 4699−4705 

Application:

HER OER EOR MOR ORR CRR ...


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